((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

Base Information

Chemical Name:((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane
CAS No.:1622235-98-6
Molecular Formula:C₂₆H₃₁BrO₂Si
Molecular Weight:483.52
Hs Code.:

Synonyms:((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

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Chemical Property of ((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

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Technology Process of ((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

There total 4 articles about ((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 14704-31-5
3-(bromomethyl)-1,1'-biphenyl

: 1622235-99-7
3-bromo-5-(((tert-butyldimethylsilyl)oxy)methyl)phenol

: 1622235-98-6
((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

Guidance literature:: 3-(bromomethyl)-1,1'-biphenyl; 3-bromo-5-(((tert-butyldimethylsilyl)oxy)methyl)phenol; With potassium carbonate; In acetone; for 24h; Reflux;

With piperazine; In acetone; for 2.5h; Reflux;

Reference yield:

: 140472-69-1
3-bromo-5-hydroxy-benzoic acid

: 1622235-98-6
((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate / acetone / 24 h / Reflux

2.2: 2.5 h / Reflux

With borane-THF; potassium carbonate; In tetrahydrofuran; acetone;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1622235-98-6
((3-([1,1′-biphenyl]-3-ylmethoxy)-5-bromobenzyl)oxy)(tertbutyl)dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: borane-THF / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: potassium carbonate / acetone / 24 h / Reflux

2.2: 2.5 h / Reflux

With borane-THF; potassium carbonate; In tetrahydrofuran; acetone;