triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

Base Information

Chemical Name:triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate
CAS No.:131166-76-2
Molecular Formula:C₆H₁₅N*C₃₄H₂₉O₁₂P
Molecular Weight:761.763
Hs Code.:

Synonyms:triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

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Chemical Property of triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

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Technology Process of triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

There total 2 articles about triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 64768-20-3,66530-18-5,113544-55-1,121530-16-3,121530-28-7,135216-27-2,101857-05-0
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

: 131166-76-2
triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

Guidance literature:: With 1H-imidazole; triethylamine; phosphorus trichloride; In acetonitrile; at 20 ℃; for 0.166667h;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 2592-58-7,3006-48-2,3006-49-3,13526-09-5,14679-57-3,22415-91-4,29884-70-6,41545-55-5,41545-56-6,41569-33-9,96996-90-6,121570-85-2,121570-86-3
1,2,3,4,6-penta-O-benzoyl-α-D-mannopyranoside

: 131166-76-2
triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / dimethylamine / acetonitrile / 5 h / 20 °C

2: 100 percent / imidazole, PCl₃, triethylamine / acetonitrile / 0.17 h / 20 °C

With 1H-imidazole; dimethyl amine; triethylamine; phosphorus trichloride; In acetonitrile;
DOI:10.1016/0008-6215(90)84021-L

Reference yield:

: 131166-76-2
triethylammonium 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl hydrogenphosphonate

: 131150-08-8
benzyl β-D-galactopyranoside 2-(α-D-mannopyranosyl phosphate), ammonium salt

Guidance literature:: Multi-step reaction with 2 steps

2: 88 percent / 0.1M MeONa / methanol; dioxane / 4 h / 1 °C

With sodium methylate; In 1,4-dioxane; methanol;
DOI:10.1016/0008-6215(90)84021-L