Technology Process of C25H27N3O8S
There total 6 articles about C25H27N3O8S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
oxalyl dichloride; C23H23N3O7S;
In
tetrahydrofuran;
at 20 ℃;
for 21h;
Inert atmosphere;
With
dimethylsulfide borane complex;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol302265z
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: manganese(IV) oxide; sodium chloride / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere
2.1: dmap / dichloromethane / 20 °C / Inert atmosphere
3.1: triethylamine; titanium tetrachloride / dichloromethane / 0 - 20 °C / Inert atmosphere
4.1: tributylphosphine / dichloromethane / 12 h / Inert atmosphere
4.2: Reflux; Inert atmosphere
5.1: tetrahydrofuran / 21 h / 20 °C / Inert atmosphere
5.2: 0.5 h / 0 °C / Inert atmosphere
With
dmap; manganese(IV) oxide; tributylphosphine; titanium tetrachloride; triethylamine; sodium chloride;
In
tetrahydrofuran; dichloromethane;
4.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol302265z
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: tributylphosphine / dichloromethane / 12 h / Inert atmosphere
1.2: Reflux; Inert atmosphere
2.1: tetrahydrofuran / 21 h / 20 °C / Inert atmosphere
2.2: 0.5 h / 0 °C / Inert atmosphere
With
tributylphosphine;
In
tetrahydrofuran; dichloromethane;
1.1: |Diels-Alder Cycloaddition;
DOI:10.1021/ol302265z
