2-PYRROLIDIN-1-YLISONICOTINONITRILE

Base Information

• Chemical Name: 2-PYRROLIDIN-1-YLISONICOTINONITRILE
• CAS No.: 127680-87-9
• Molecular Formula: C10H11 N3
• Molecular Weight: 173.217
• Hs Code.: 2933990090
• Mol file: 127680-87-9.mol

Synonyms:2-PYRROLIDIN-1-YLISONICOTINONITRILE;2-(Pyrrolidin-1-yl)isonicotinonitrile 97%

Chemical Property of 2-PYRROLIDIN-1-YLISONICOTINONITRILE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 79 °C
• Boiling Point: 328.7°Cat760mmHg
• Flash Point: 152.6°C
• PSA: 39.92000
• Density: 1.18g/cm³
• LogP: 1.61848
• Storage Temp.: 2-8°C

Purity/Quality:

98%min ^*data from raw suppliers

2-Pyrrolidin-1-ylisonicotinonitrile ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-PYRROLIDIN-1-YLISONICOTINONITRILE

There total 1 articles about 2-PYRROLIDIN-1-YLISONICOTINONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyrrolidine (123-75-1) + 2,4-Dicyanopyridine (29181-50-8) → 2-Cyanopyridine (100-70-9,1232006-36-8) + 4-pyrrolidinopicolinonitrile (127680-86-8) + 2-Pyrrolidin-1-yl-isonicotinonitrile (127680-87-9)

Guidance literature:

In water; acetonitrile; for 2.5h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1039/P19900000097

upstream raw materials:

pyrrolidine

2,4-Dicyanopyridine

Refernces

• 1、 Bernardi, Rosanna,Caronna, Tullio,Morrocchi, Sergio,Ursini, Maurizio,Vittimberga, Bruno M.. "A Study of the Photochemically Induced Reaction of Pyridine-2,4-dicarbonitrile with Primary and Secondary Amines. A Direct Synthesis of Aminocyanopyridines". . p. 97 - 100. Retrieved 2007/10/02.