3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

Base Information

Chemical Name:3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline
CAS No.:118683-77-5
Molecular Formula:C₁₉H₂₃NO₅S
Molecular Weight:377.461
Hs Code.:

Synonyms:3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

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Chemical Property of 3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

Chemical Property:

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Technology Process of 3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

There total 6 articles about 3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 124-63-0
methanesulfonyl chloride

: 104013-60-7
3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>aniline

: 118683-77-5
3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

Guidance literature:: With pyridine; In dichloromethane; for 0.166667h; Ambient temperature;

Reference yield:

: 40786-69-4
1-(2,4-dihydroxy-3-propylphenyl)ethanone

: 118683-77-5
3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / K₂CO₃ / acetone / 12 h / Heating

2: 82 percent / CF₃CO₂H / CH₂Cl₂ / 1.5 h / Ambient temperature

3: 51 percent / pyridine / CH₂Cl₂ / 0.17 h / Ambient temperature

With pyridine; potassium carbonate; trifluoroacetic acid; In dichloromethane; acetone;

Reference yield:

: 1877-77-6
3-aminobenzenemethanol

: 118683-77-5
3-<(4-acetyl-3-hydroxy-2-propylphenoxy)methyl>-N-(methylsulfonyl)aniline

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / tetrahydrofuran / 5 h / Heating

2: 74 percent / CBr₄, Ph₃P / CH₂Cl₂ / 1.5 h / 0 °C

3: 92 percent / K₂CO₃ / acetone / 12 h / Heating

4: 82 percent / CF₃CO₂H / CH₂Cl₂ / 1.5 h / Ambient temperature

5: 51 percent / pyridine / CH₂Cl₂ / 0.17 h / Ambient temperature

With pyridine; carbon tetrabromide; potassium carbonate; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; acetone;