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methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside

Base Information Edit
  • Chemical Name:methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside
  • CAS No.:103456-59-3
  • Molecular Formula:C27H30O4
  • Molecular Weight:418.533
  • Hs Code.:
  • Mol file:103456-59-3.mol
methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside

Synonyms:methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside

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Chemical Property of methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside Edit
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Technology Process of methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside

There total 1 articles about methyl 2,4-dideoxy-3-O-methyl-6-O-trityl-α-D-erythro-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: 79 percent / sodium, ammonia / tetrahydrofuran / 1) -78 deg C, 30 min, 2) reflux, 30 min
2: 96 percent / pyridine / 11 h / Ambient temperature
With pyridine; ammonia; sodium; In tetrahydrofuran;
DOI:10.1021/ja00279a041
Guidance literature:
Multi-step reaction with 10 steps
1: 79 percent / sodium, ammonia / tetrahydrofuran / 1) -78 deg C, 30 min, 2) reflux, 30 min
2: 96 percent / pyridine / 11 h / Ambient temperature
3: 96 percent / sodium iodide / butan-2-one / 4 h / Heating; in dark
4: 90 percent / sodium hydride (56.8percent oil dispersion) / dimethylsulfoxide / 9 h
5: 92 percent / sodium phosphate, sodium amalgam / methanol / 0.25 h
6: 100 percent / lithium aluminum hydride / diethyl ether / 0.25 h
7: 90 percent / pyridine, chromium trioxide / CH2Cl2 / 0.33 h / 0 °C
8: 1) n-butyllithium, 2) tetrabutylammonium fluoride / 1) THF, hexane, RT, 1 h, 2) THF, 10 min
9: hexamethylphosphoramide, 2,2'-dimethyl-2,2'-azopropionitrile / 0.08 h
10: 2,6-di-tert-butyl-4-methylphenol / toluene / 14 h / 125 °C
With pyridine; chromium(VI) oxide; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium amalgam; lithium aluminium tetrahydride; n-butyllithium; 2,2'-azobis(isobutyronitrile); 2,6-di-tert-butyl-4-methyl-phenol; tetrabutyl ammonium fluoride; ammonia; sodium; sodium hydride; sodium phosphate; sodium iodide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; dimethyl sulfoxide; toluene; butanone;
DOI:10.1021/ja00279a041
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