3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

Base Information

Chemical Name:3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester
CAS No.:103777-49-7
Molecular Formula:C₃₅H₃₆O₈
Molecular Weight:584.666
Hs Code.:

Synonyms:3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

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Chemical Property of 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

Chemical Property:

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Technology Process of 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

There total 1 articles about 3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6962-57-8
3,6-dihydroxy-2,4-dimethoxyacetophenone

: 103777-49-7
3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / Heating

2: pyridine / 3 h / 120 °C

With pyridine; potassium carbonate; In acetone;
DOI:10.1021/jm00161a021

Reference yield:

: 103777-49-7
3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

: 103776-90-5
6-Butoxy-2-(3,4-dihydroxy-phenyl)-5-hydroxy-7-methoxy-chromen-4-one

Guidance literature:: Multi-step reaction with 6 steps

1: KOH, pyridine / 4 h / 60 °C

2: 73 percent / AcONa, AcOH / 3 h / 140 - 145 °C

3: 91 percent / H₂ / 10percent Pd/C / methanol; ethyl acetate

4: pyridine / Heating

5: AlCl₃ / acetonitrile / 1.5 h / 60 °C

6: 6 M HCl / methanol / 4 h / Heating

With pyridine; hydrogenchloride; potassium hydroxide; aluminium trichloride; hydrogen; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate; acetonitrile;
DOI:10.1021/jm00161a021

Reference yield:

: 103777-49-7
3,4-Bis-benzyloxy-benzoic acid 2-acetyl-4-butoxy-3,5-dimethoxy-phenyl ester

: 103776-58-5
6-Butoxy-2-(3,4-dihydroxy-phenyl)-5,7-dimethoxy-chromen-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: KOH, pyridine / 4 h / 60 °C

2: 73 percent / AcONa, AcOH / 3 h / 140 - 145 °C

3: 91 percent / H₂ / 10percent Pd/C / methanol; ethyl acetate

With pyridine; potassium hydroxide; hydrogen; sodium acetate; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00161a021