3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

Base Information

Chemical Name:3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde
CAS No.:355019-18-0
Molecular Formula:C₁₆H₁₉NO₂
Molecular Weight:257.332
Hs Code.:

Synonyms:3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

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Chemical Property of 3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

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Technology Process of 3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

There total 1 articles about 3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2579-22-8
Phenylpropargyl aldehyde

: 4567-18-4
2,5,5-trimethylpyrroline N-oxide

: 355019-18-0
3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

Guidance literature:: In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(01)00322-2

Reference yield: 94.0%

: 106-95-6
allyl bromide

: 355019-18-0
3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

: 1-(3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-yl)but-3-en-1-ol

Guidance literature:: In tetrahydrofuran; diethyl ether; at 0 ℃;
DOI:10.1016/S0040-4020(01)00322-2

Reference yield: 74.0%

: 21752-80-7
1,3-bis(trimethylsilyl)propyne

: 355019-18-0
3a,6,6-trimethyl-2-phenyl-3a,4,5,6-tetrahydropyrrolo[1,2-b]isoxazol-3-carbaldehyde

: 428516-73-8
(Z)-3a,4,5,6-tetrahydro-3a,6,6-trimethyl-2-phenyl-3-[4-(trimethylsilyl)but-1-en-3-ynyl]pyrrolo[1,2-b]isoxazole

: (E)-3a,4,5,6-tetrahydro-3a,6,6-trimethyl-2-phenyl-3-[4-(trimethylsilyl)but-1-en-3-ynyl]pyrrolo[1,2-b]isoxazole

Guidance literature:: With titanium(IV) isopropylate; n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 1.75h;
DOI:10.1002/1522-2675(20011219)84:12<3822::AID-HLCA3822>3.0.CO;2-O