N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

Base Information

Chemical Name:N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine
CAS No.:110915-93-0
Molecular Formula:C₁₅H₂₆N₂O
Molecular Weight:250.384
Hs Code.:

N<sup>1</sup>-(2,6-Dimethyl-phenyl)-N<sup>2</sup>-(2-methoxy-ethyl)-N<sup>2</sup>-methyl-propane-1,2-diamine

Synonyms:N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

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Chemical Property of N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

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Technology Process of N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

There total 3 articles about N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110916-01-3
N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

: 110915-93-0
N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

Guidance literature:: With ammonia; sodium; In isopropyl alcohol; toluene; at -40 - -35 ℃; for 2h;

Reference yield:

: 66236-09-7
N-(2,6-dimethylphenyl)-methane sulfonamide

: 110915-93-0
N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

2: 88 percent / pyridine / 3 h / 0 - 5 °C

3: 79 percent / ethanol / 120 - 125 °C / steel bomb

4: 53 percent / NaH / dimethylsulfoxide / 2 h / 25 °C

5: 80 percent / liq. NH₃, Na / toluene; propan-2-ol / 2 h / -40 - -35 °C

With pyridine; sodium hydroxide; ammonia; sodium; sodium hydride; In ethanol; dimethyl sulfoxide; isopropyl alcohol; toluene;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 110915-93-0
N¹-(2,6-Dimethyl-phenyl)-N²-(2-methoxy-ethyl)-N²-methyl-propane-1,2-diamine

Guidance literature:: Multi-step reaction with 6 steps

1: 91 percent

2: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

3: 88 percent / pyridine / 3 h / 0 - 5 °C

4: 79 percent / ethanol / 120 - 125 °C / steel bomb

5: 53 percent / NaH / dimethylsulfoxide / 2 h / 25 °C

6: 80 percent / liq. NH₃, Na / toluene; propan-2-ol / 2 h / -40 - -35 °C

With pyridine; sodium hydroxide; ammonia; sodium; sodium hydride; In ethanol; dimethyl sulfoxide; isopropyl alcohol; toluene;