N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

Base Information

Chemical Name:N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide
CAS No.:110916-01-3
Molecular Formula:C₁₆H₂₈N₂O₃S
Molecular Weight:328.476
Hs Code.:

Synonyms:N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

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Chemical Property of N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

Chemical Property:

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Technology Process of N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

There total 5 articles about N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 110916-00-2
N-(2,6-Dimethyl-phenyl)-N-{2-[(2-hydroxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

: 74-88-4
methyl iodide

: 110916-01-3
N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

Guidance literature:: With sodium hydride; In dimethyl sulfoxide; at 25 ℃; for 2h;

Reference yield:

: 66236-09-7
N-(2,6-dimethylphenyl)-methane sulfonamide

: 110916-01-3
N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

2: 88 percent / pyridine / 3 h / 0 - 5 °C

3: 79 percent / ethanol / 120 - 125 °C / steel bomb

4: 53 percent / NaH / dimethylsulfoxide / 2 h / 25 °C

With pyridine; sodium hydroxide; sodium hydride; In ethanol; dimethyl sulfoxide;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 110916-01-3
N-(2,6-Dimethyl-phenyl)-N-{2-[(2-methoxy-ethyl)-methyl-amino]-propyl}-methanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent

2: 70 percent / 0.5N NaOH / 1) 80 - 85 deg C, 4 h, 2) RT, overnight

3: 88 percent / pyridine / 3 h / 0 - 5 °C

4: 79 percent / ethanol / 120 - 125 °C / steel bomb

5: 53 percent / NaH / dimethylsulfoxide / 2 h / 25 °C

With pyridine; sodium hydroxide; sodium hydride; In ethanol; dimethyl sulfoxide;