3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Base Information

Chemical Name:3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol
CAS No.:216968-18-2
Molecular Formula:C₇₉H₁₀₄O₁₄
Molecular Weight:1277.69
Hs Code.:

3-[3,5-bis-(3-{3,5-bis-[3-(4-<i>tert</i>-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Synonyms:3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Suppliers and Price of 3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

There total 8 articles about 3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 176216-57-2
1-(3-Bromo-propoxy)-3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-benzene

: 216968-13-7
5-(3-hydroxypropyloxy)-1,3-resorcinol

: 216968-18-2
3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Guidance literature:: With 18-crown-6 ether; potassium carbonate; In tetrahydrofuran; for 24h; Heating;
DOI:10.1016/S0040-4020(98)00851-5

Reference yield:

: 108-73-6
3,5-dihydroxyphenol

: 216968-18-2
3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 59 percent / K₂CO₃ / dimethylformamide / 48 h / 20 °C

2: 73 percent / ethanethiol; sodium hydride / dimethylformamide / 5 h / 0 - 150 °C

3: 89 percent / K₂CO₃ / acetone / 24 h / Heating

4: 76 percent / H₂ / Pd/C / ethanol; ethyl acetate / 20 °C

5: 91 percent / 18-crown-6; K₂CO₃ / tetrahydrofuran / 24 h / Heating

6: 96 percent / CBr₄; PPh₃ / tetrahydrofuran / 12 h / 20 °C

7: 86 percent / 18-crown-6; K₂CO₃ / tetrahydrofuran / 24 h / Heating

With 18-crown-6 ether; carbon tetrabromide; hydrogen; sodium hydride; potassium carbonate; triphenylphosphine; ethanethiol; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide; acetone; 1: Alkylation / 2: debenzylation / 3: Alkylation / 4: Hydrogenolysis / 5: Alkylation / 6: Bromination / 7: Alkylation;
DOI:10.1016/S0040-4020(98)00851-5

Reference yield:

: 59434-20-7
1,3,5-tri-O-benzylphloroglucinol

: 216968-18-2
3-[3,5-bis-(3-{3,5-bis-[3-(4-tert-butyl-phenoxy)-propoxy]-phenoxy}-propoxy)-phenoxy]-propan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 73 percent / ethanethiol; sodium hydride / dimethylformamide / 5 h / 0 - 150 °C

2: 89 percent / K₂CO₃ / acetone / 24 h / Heating

3: 76 percent / H₂ / Pd/C / ethanol; ethyl acetate / 20 °C

4: 91 percent / 18-crown-6; K₂CO₃ / tetrahydrofuran / 24 h / Heating

5: 96 percent / CBr₄; PPh₃ / tetrahydrofuran / 12 h / 20 °C

6: 86 percent / 18-crown-6; K₂CO₃ / tetrahydrofuran / 24 h / Heating

With 18-crown-6 ether; carbon tetrabromide; hydrogen; sodium hydride; potassium carbonate; triphenylphosphine; ethanethiol; palladium on activated charcoal; In tetrahydrofuran; ethanol; ethyl acetate; N,N-dimethyl-formamide; acetone; 1: debenzylation / 2: Alkylation / 3: Hydrogenolysis / 4: Alkylation / 5: Bromination / 6: Alkylation;
DOI:10.1016/S0040-4020(98)00851-5