C₁₄H₁₆FN₇O₂

Base Information

Chemical Name:C₁₄H₁₆FN₇O₂
CAS No.:1334167-81-5
Molecular Formula:C₁₄H₁₆FN₇O₂
Molecular Weight:333.325
Hs Code.:

C<sub>14</sub>H<sub>16</sub>FN<sub>7</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₆FN₇O₂

Suppliers and Price of C₁₄H₁₆FN₇O₂

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₄H₁₆FN₇O₂

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₄H₁₆FN₇O₂

There total 9 articles about C₁₄H₁₆FN₇O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1219707-39-7
delpazolid

: 1334167-81-5
C₁₄H₁₆FN₇O₂

Guidance literature:: With di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; triphenylphosphine; In tetrahydrofuran; at 0 ℃; for 1.5h;

Reference yield:

: 509151-97-7
2-(2-fluoro-4-nitrophenylamino)ethanol

: 1334167-81-5
C₁₄H₁₆FN₇O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / dichloromethane / 0.5 h / 0 °C

2.1: N-ethyl-N,N-diisopropylamine / ethanol; water / 2 h / Reflux

3.1: acetic acid / 15 h / Reflux

3.2: pH 8 - 9

4.1: hydrogen / palladium-on-charcoal / methanol / 4 h / 20 °C

5.1: dichloromethane / 3 h / 20 °C

5.2: 4 h / 50 °C

6.1: lithium tert-butoxide; methanol / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

6.2: 10 h / 20 °C

7.1: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

With methanol; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; palladium-on-charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 1334167-81-5
C₁₄H₁₆FN₇O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: acetonitrile / 4 h / Reflux

2.1: triethylamine / dichloromethane / 0.5 h / 0 °C

3.1: N-ethyl-N,N-diisopropylamine / ethanol; water / 2 h / Reflux

4.1: acetic acid / 15 h / Reflux

4.2: pH 8 - 9

5.1: hydrogen / palladium-on-charcoal / methanol / 4 h / 20 °C

6.1: dichloromethane / 3 h / 20 °C

6.2: 4 h / 50 °C

7.1: lithium tert-butoxide; methanol / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C

7.2: 10 h / 20 °C

8.1: triphenylphosphine; diphenyl phosphoryl azide; di-isopropyl azodicarboxylate / tetrahydrofuran / 1.5 h / 0 °C

With methanol; di-isopropyl azodicarboxylate; diphenyl phosphoryl azide; hydrogen; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium tert-butoxide; palladium-on-charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;