4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

Base Information

Chemical Name:4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate
CAS No.:1352087-18-3
Molecular Formula:C₂₈H₃₄N₂O₅Si
Molecular Weight:506.674
Hs Code.:

Synonyms:4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

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Chemical Property of 4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

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Technology Process of 4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

There total 3 articles about 4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352087-17-2
3-(tert-butyldiphenylsilanoxy)-2,2-dimethyl-propylamine

: 7693-46-1
4-Nitrophenyl chloroformate

: 1352087-18-3
4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 1.75h;

Reference yield:

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1352087-18-3
4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.75 h / 0 °C

With dmap; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield:

: 26734-09-8
3-amino-2,2-dimethylpropan-1-ol

: 1352087-18-3
4-nitrophenyl 3-(tert-butyldiphenylsilanoxy)-2,2-dimethylpropylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; triethylamine / dichloromethane / 2.5 h / 0 - 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 1.75 h / 0 °C

With dmap; triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane;