benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

Base Information

Chemical Name:benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside
CAS No.:1608472-11-2
Molecular Formula:C₄₂H₄₁ClO₆
Molecular Weight:677.237
Hs Code.:

Synonyms:benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

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Chemical Property of benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

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Technology Process of benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

There total 2 articles about benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 1094382-79-2
1,5-anhydro-2,3,4,6-tetra-O-benzyl-1,2-C-(dichloromethylene)-α-D-glycero-D-galacto-hexitol

: 563-63-3
silver(I) acetate

: 100-51-6,185532-71-2
benzyl alcohol

: 1608472-11-2
benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

: 1608472-12-3
acetyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabinohept-2-enoseptanoside

Guidance literature:: In toluene; for 72h; Reflux;
DOI:10.1016/j.carres.2014.01.023

Reference yield:

: 4132-26-7
2,3,4,6-tetra-O-benzyl 1,5-anhydro-D-arabino-hex-1-enitol

: 1608472-11-2
benzyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabino-hept-2-enoseptanoside

: 1608472-12-3
acetyl 2-chloro-2-deoxy-3,4,5,7-tetra-O-benzyl-α-D-arabinohept-2-enoseptanoside

Guidance literature:: Multi-step reaction with 2 steps

1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water / 6 h / 20 °C

2: toluene / 72 h / Reflux

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; toluene;
DOI:10.1016/j.carres.2014.01.023