[4-(3-Methyoxypropoxy)-3-methyl-2-pyridinyl]methanol hydrochloride

Base Information

• Chemical Name: [4-(3-Methyoxypropoxy)-3-methyl-2-pyridinyl]methanol hydrochloride
• CAS No.: 675198-19-3
• Molecular Formula: C11H17NO3^.HCl
• Molecular Weight: 247.722
• Mol file: 675198-19-3.mol

Synonyms:2-Pyridinemethanol,4-(3-methoxypropoxy)-3-methyl-, hydrochloride (9CI);2-Hydroxymethyl-4-(3-methoxypropoxy)-3-methylpyridinehydrochloride;[4-(3-Methoxypropoxy)-3-methylpyridin-2-yl]methanolhydrochloride;

Chemical Property of [4-(3-Methyoxypropoxy)-3-methyl-2-pyridinyl]methanol hydrochloride

Chemical Property:

• PSA: 51.58000
• LogP: 2.09960
• Storage Temp.: Inert atmosphere,Room Temperature
• Solubility.: Chloroform (Slightly), Methanol (Slightly)

Purity/Quality:

98%, ^*data from raw suppliers

(4-(3-Methoxypropoxy)-3-methylpyridin-2-yl)methanolHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of [4-(3-Methyoxypropoxy)-3-methyl-2-pyridinyl]methanol hydrochloride

There total 4 articles about [4-(3-Methyoxypropoxy)-3-methyl-2-pyridinyl]methanol hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-2,3-dimethylpyridine-N-oxide (59886-90-7) → [4-(3-methoxypropoxy)-3-methylpyridin-2-yl]methanol hydrochloride (675198-19-3)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide

2: acetic acid / methanol; toluene

3: sodium hydroxide / methanol

With acetic acid; sodium hydroxide; In methanol; toluene;

DOI:10.14233/ajchem.2013.14818

Reference yield:

2-acetoxymethyl-4-(3-methoxy propoxy)-3-methyl pyridine → [4-(3-methoxypropoxy)-3-methylpyridin-2-yl]methanol hydrochloride (675198-19-3)

Guidance literature:

With sodium hydroxide; In methanol;

DOI:10.14233/ajchem.2013.14818

Reference yield:

2,3-dimethyl-4-nitropyridine N-oxide (37699-43-7) → [4-(3-methoxypropoxy)-3-methylpyridin-2-yl]methanol hydrochloride (675198-19-3)

Guidance literature:

Multi-step reaction with 4 steps

1: trichlorophosphate / Reflux

2: sodium hydroxide

3: acetic acid / methanol; toluene

4: sodium hydroxide / methanol

With acetic acid; sodium hydroxide; trichlorophosphate; In methanol; toluene;

DOI:10.14233/ajchem.2013.14818

upstream raw materials:

2,3-dimethyl-4-nitropyridine N-oxide

4-chloro-2,3-dimethylpyridine-N-oxide

2,3-dimethyl-4-(3-methoxypropoxy)pyridine nitroxide

Downstream raw materials:

rabeprazole

rabeprazole sulfide

2-chloromethyl-4-(3-methoxy propyloxy)-3-methyl pyridine

Rabeprazole sodium

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