tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Base Information

Chemical Name:tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate
CAS No.:1345958-90-8
Molecular Formula:C₂₁H₃₂N₂O₃S
Molecular Weight:392.563
Hs Code.:

Synonyms:tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

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Chemical Property of tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

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Technology Process of tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

There total 2 articles about tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345958-89-5
tert-butyl 4-{4-[methoxy(methyl)carbamoyl]-1,3-thiazol-2-yl}piperidine-1-carboxylate

: 32936-61-1
(cyclohexylmethyl)magnesium chloride

: 1345958-90-8
tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Guidance literature:: tert-butyl 4-{4-[methoxy(methyl)carbamoyl]-1,3-thiazol-2-yl}piperidine-1-carboxylate; (cyclohexylmethyl)magnesium chloride; In tetrahydrofuran; diethyl ether; at -78 - 20 ℃; for 2h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 365413-00-9
4-(4-carboxy-thiazol-2-yl)-piperidine-1-carboxylic acid tert-butyl ester

: 1345958-90-8
tert-butyl 4-[4-(cyclohexylacetyl)-1,3-thiazol-2-yl]piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.17 h / 20 °C

1.2: 20 °C

2.1: diethyl ether; tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere

With triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane;