methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate

Base Information

• Chemical Name: methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate
• CAS No.: 956580-53-3
• Molecular Formula: C₂₆H₂₅NO₃
• Molecular Weight: 399.489

Synonyms:methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate

Chemical Property of methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate

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Technology Process of methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate

There total 1 articles about methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-cyclohexyl-2-[2-(hydroxymethyl)phenyl]-1-prop-2-yn-1-yl-1H-indole-6-carboxylate (956580-52-2) → methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate (956580-53-3)

Guidance literature:

With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -70 ℃; for 0.5h;

methyl 3-cyclohexyl-2-[2-(hydroxymethyl)phenyl]-1-prop-2-yn-1-yl-1H-indole-6-carboxylate; In dichloromethane; at -70 ℃; for 0.5h;

With triethylamine; In dichloromethane; at 0 ℃; for 0.333333h;

Reference yield:

methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate (956580-53-3) + N-(2-tert-butoxycarbonylaminoethyl)aminoacetic acid (90495-99-1) → methyl-1-{2-[(tert-butoxycarbonyl)amino]ethyl}-10-cyclohexyl-1,4-dihydroindolo[2,1-a]pyrrolo[3,2-d][2]benzazepine-7-carboxylate + methyl-1-{2-[(tert-butoxycarbonyl)amino]ethyl}-10-cyclohexyl-1,2,4,14b-tetrahydroindolo[2,1-a]pyrrolo[3,2-d][2]benzazepine-7-carboxylate

Guidance literature:

In toluene; at 140 ℃; for 6h;

Reference yield:

methyl 3-cyclohexyl-2-(2-formylphenyl)-1-prop-2-yn-1-yl-1H-indole-6-carboxylate (956580-53-3) + glycine (56-40-6,18875-39-3,25718-94-9) → C27H28N2O2

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 140 ℃;

DOI:10.1016/j.bmcl.2008.12.039

upstream raw materials:

methyl 3-cyclohexyl-2-[2-(hydroxymethyl)phenyl]-1-prop-2-yn-1-yl-1H-indole-6-carboxylate

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