C₂₆H₃₁N₅O₄

Base Information

Chemical Name:C₂₆H₃₁N₅O₄
CAS No.:1346243-04-6
Molecular Formula:C₂₆H₃₁N₅O₄
Molecular Weight:477.563
Hs Code.:

C<sub>26</sub>H<sub>31</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₆H₃₁N₅O₄

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Chemical Property of C₂₆H₃₁N₅O₄

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Technology Process of C₂₆H₃₁N₅O₄

There total 6 articles about C₂₆H₃₁N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.5%

: 930-37-0
glycidyl methyl ether

: 1346245-07-5
C₂₂H₂₃N₅O₂

: 1346243-04-6
C₂₆H₃₁N₅O₄

Guidance literature:: C₂₂H₂₃N₅O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 5 ℃; for 1h; Inert atmosphere;

glycidyl methyl ether; In N,N-dimethyl-formamide; mineral oil; at 5 - 80 ℃; Inert atmosphere;

Reference yield:

: 10272-07-8
3.5-dimethoxyaniline

: 1346243-04-6
C₂₆H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

4.2: 5 - 80 °C / Inert atmosphere

With potassium phosphate; sodium hydride; sodium t-butanolate; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 82031-32-1
7-bromo-1H-quinoxalin-2-one

: 1346243-04-6
C₂₆H₃₁N₅O₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium t-butanolate / palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux

2.1: trichlorophosphate / 0.67 h / 80 °C

3.1: potassium phosphate / tetrakis(triphenylphosphine) palladium⁽⁰⁾; XPhos / 1,4-dioxane; water / 80 °C / Inert atmosphere

4.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 5 °C / Inert atmosphere

4.2: 5 - 80 °C / Inert atmosphere

With potassium phosphate; sodium hydride; sodium t-butanolate; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; XPhos; In 1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide; mineral oil;