methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

Base Information

Chemical Name:methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate
CAS No.:934664-26-3
Molecular Formula:C₁₃H₁₁FIN₃O₃
Molecular Weight:403.152
Hs Code.:

Synonyms:methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

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Chemical Property of methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

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Technology Process of methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

There total 2 articles about methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 8.7%

: 67-56-1
methanol

: 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carbonyl chloride

: 934664-26-3
methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

Guidance literature:: With diazomethyl-trimethyl-silane; In benzene; at 20 ℃; for 0.25h;

Reference yield: 8.7%

: 67-56-1
methanol

: 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carbonyl chloride

: 18107-18-1
diazomethyl-trimethyl-silane

: 934664-26-3
methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

Guidance literature:: methanol; 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carbonyl chloride; diazomethyl-trimethyl-silane; In benzene; at 20 ℃; for 0.25h;

With acetic acid; In methanol; benzene;

Reference yield: 66.0%

: 934664-26-3
methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate

: 934664-24-1
4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylic acid

Guidance literature:: methyl 4-(2-fluoro-4-iodophenylamino)-1-methyl-6-oxo-1,6-dihydropyridazine-3-carboxylate; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 - 50 ℃; for 16.6667h;

With hydrogenchloride; In water; pH=2; Product distribution / selectivity; Acidic aqueous solution;