acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

Base Information

Chemical Name:acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester
CAS No.:1215855-23-4
Molecular Formula:C₂₈H₂₉N₃O₅
Molecular Weight:487.555
Hs Code.:

Synonyms:acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

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Chemical Property of acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

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Technology Process of acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

There total 7 articles about acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1215855-22-3
2-(3-acetoxybenzoylamino)-acetic acid

: 144881-52-7
1-(4-benzyloxyphenyl)piperazine

: 1215855-23-4
acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

Guidance literature:: 2-(3-acetoxybenzoylamino)-acetic acid; With triethylamine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃;

1-(4-benzyloxyphenyl)piperazine; With triethylamine; In tetrahydrofuran; dichloromethane; at 10 - 20 ℃;

Reference yield:

: C₁₆H₁₉NO₇

: 144881-52-7
1-(4-benzyloxyphenyl)piperazine

: 1215855-23-4
acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; dichloromethane; at 10 - 20 ℃;

Reference yield:

: 1215855-21-2
(3-acetoxy-benzoylamino)-acetic acid benzyl ester

: 1215855-23-4
acetic acid 3-{2-[4-(4-benzyloxy-phenyl)-piperazin-1-yl]-2-oxo-ethylcarbamoyl}-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 20 °C

2: triethylamine / tetrahydrofuran / -15 °C

3: triethylamine / dichloromethane; tetrahydrofuran / 10 - 20 °C

With hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; dichloromethane;