o-allylphenylmagnesium bromide

Base Information

• Chemical Name: o-allylphenylmagnesium bromide
• CAS No.: 65273-28-1
• Molecular Formula: C₉H₉BrMg
• Molecular Weight: 221.379

Synonyms:o-allylphenylmagnesium bromide

Chemical Property of o-allylphenylmagnesium bromide

Chemical Property:

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Technology Process of o-allylphenylmagnesium bromide

There total 1 articles about o-allylphenylmagnesium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1-allyl-2-bromobenzene (42918-20-7) → o-allylphenylmagnesium bromide (65273-28-1)

Guidance literature:

With magnesium; In diethyl ether; for 0.333333h;

Reference yield: 79.0%

(tricyclohexylphosphine)gold(I) chloride (49763-41-9) + o-allylphenylmagnesium bromide (65273-28-1) → Cy3PAu(2-(CH2CH=CH2)C6H4)

Guidance literature:

In tetrahydrofuran; at -78 - 0 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja503974x

Reference yield: 73.0%

3-methoxycyclohex-2-en-1-one (16807-60-6) + o-allylphenylmagnesium bromide (65273-28-1) → 2’-allyl-5,6-dihydro-[1,1‘-biphenyl]-3(4H)-one (90930-90-8)

Guidance literature:

DOI:10.1039/c39840000322

upstream raw materials:

1-allyl-2-bromobenzene

Downstream raw materials:

2’-allyl-5,6-dihydro-[1,1‘-biphenyl]-3(4H)-one

3-(2-Allyl-phenyl)-5-methyl-cyclohex-2-enone

3-(2-Allyl-phenyl)-cyclohex-2-enol

2-[1-(2-Allyl-phenyl)-cyclohex-2-enyl]-N,N-dimethyl-acetamide

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