N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Base Information

Chemical Name:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide
CAS No.:1449203-98-8
Molecular Formula:C₁₅H₁₈IN₃O₃S
Molecular Weight:447.297
Hs Code.:

Synonyms:N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Suppliers and Price of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

There total 6 articles about N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.66%

: C₂₁H₂₈IN₃O₄S

: 1449203-98-8
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Guidance literature:: With methanol; sodium hydroxide; for 3h; Reflux;

Reference yield:

: 5438-36-8
5-iodovaniline

: 1449203-98-8
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / 20 °C

2.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

3.1: iron(III) chloride / methanol; water / Reflux

3.2: 1 h / Reflux

4.1: pyridine / 2 h / 20 °C

5.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; sulfuric acid; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001

Reference yield:

: 486994-14-3
4-(acetyloxy)-3-iodo-5-methoxybenzaldehyde

: 1449203-98-8
N-[5-(4-hydroxy-5-methoxy-3-iodophenyl)-1,3,4-thiadiazole-2-yl] hexanamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / methanol / 6 h / pH 4 - 5 / Reflux

2.1: iron(III) chloride / methanol; water / Reflux

2.2: 1 h / Reflux

3.1: pyridine / 2 h / 20 °C

4.1: sodium hydroxide / methanol / 3 h / Reflux

With pyridine; iron(III) chloride; acetic acid; sodium hydroxide; In methanol; water;
DOI:10.1016/j.ejmech.2013.05.001