(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

Base Information

Chemical Name:(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide
CAS No.:1616405-40-3
Molecular Formula:C₁₇H₁₅N₃O₄S
Molecular Weight:357.39
Hs Code.:

Synonyms:(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

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Technology Process of (E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

There total 4 articles about (E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1616405-30-1
N-methyl-4-nitro-N-((1-tosyl-1H-1,2,3-triazol-4-yl)methyl)aniline

: 1616405-40-3
(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

Guidance literature:: With rhodium (II) octanoate dimer; In 1,2-dichloro-ethane; at 60 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol501618z

Reference yield:

: 75077-46-2
4-nitro-N-2-propynylbenzenamine

: 1616405-40-3
(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

2: copper(I) thiophene-2-carboxylate / toluene / 2 h / 20 °C / Inert atmosphere

3: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / 60 °C / Inert atmosphere

With copper(I) thiophene-2-carboxylate; rhodium (II) octanoate dimer; potassium carbonate; In 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501618z

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1616405-40-3
(E)-4-methyl-N-((1-methyl-5-nitro-1H-indol-3-yl)methylene)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / toluene; dichloromethane / 14 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 0 - 20 °C / Inert atmosphere

3: copper(I) thiophene-2-carboxylate / toluene / 2 h / 20 °C / Inert atmosphere

4: rhodium (II) octanoate dimer / 1,2-dichloro-ethane / 6 h / 60 °C / Inert atmosphere

With copper(I) thiophene-2-carboxylate; rhodium (II) octanoate dimer; potassium carbonate; In dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol501618z