Boc-D-Phe-OAll

Base Information

• Chemical Name: Boc-D-Phe-OAll
• CAS No.: 876396-82-6
• Molecular Formula: C₁₇H₂₃NO₄
• Molecular Weight: 305.374
• Mol file: 876396-82-6.mol

Synonyms:Boc-D-Phe-OAll

Chemical Property of Boc-D-Phe-OAll

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Boc-D-Phe-OAll

There total 4 articles about Boc-D-Phe-OAll which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

C14H18NO4(1-)*Na(1+) (1013327-78-0) + allyl alcohol (107-18-6) → Boc-D-Phe-OAll (876396-82-6)

Guidance literature:

With tetra-(n-butyl)ammonium iodide; triethylamine; In N,N-dimethyl-formamide; for 7h; Heating;

DOI:10.1016/j.tetlet.2007.12.068

Reference yield:

Boc-D-Phe-OH (18942-49-9) + allyl bromide (106-95-6) → Boc-D-Phe-OAll (876396-82-6)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; for 4h;

DOI:10.1021/acs.orglett.9b02592

Reference yield:

Boc-D-Phe-OH (18942-49-9) + allyl alcohol (107-18-6) → Boc-D-Phe-OAll (876396-82-6)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane;

DOI:10.1021/ol5023118

upstream raw materials:

C₁₄H₁₈NO₄^(1-)*Na⁽¹⁺⁾

allyl alcohol

Boc-D-Phe-OH

allyl bromide