C₉⁽¹³⁾CH₁₀O₂

Base Information

• Chemical Name: C₉⁽¹³⁾CH₁₀O₂
• CAS No.: 88058-20-2
• Molecular Formula: C₁₀H₁₀O₂
• Molecular Weight: 163.177
• Mol file: 88058-20-2.mol

Synonyms:C₉⁽¹³⁾CH₁₀O₂

Chemical Property of C₉⁽¹³⁾CH₁₀O₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₉⁽¹³⁾CH₁₀O₂

There total 2 articles about C₉⁽¹³⁾CH₁₀O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

methanol (67-56-1) + <1-13C>-(Z)-cinnamic acid (74895-25-3) → C9(13)CH10O2 (88058-20-2)

Guidance literature:

With toluene-4-sulfonic acid; at 70 ℃; for 10h;

DOI:10.1039/P29800001028

Reference yield:

<1-13C>-3-phenylpropynoic acid (61633-35-0) → C9(13)CH10O2 (88058-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 68 percent / H₂ / Lindlar catalyst / hexane

2: 70 percent / toluene-p-sulphonic acid / 10 h / 70 °C

With hydrogen; toluene-4-sulfonic acid; Lindlar's catalyst; In hexane;

DOI:10.1039/P29800001028

Reference yield: 84.0%

C9(13)CH10O2 (88058-20-2) → <1-13C>-(E)-methyl cinnamate (74895-26-4)

Guidance literature:

With iodine; In hexane; at 70 ℃; for 144h;

DOI:10.1039/P29800001028

upstream raw materials:

methanol

<1-13C>-(Z)-cinnamic acid

<1-13C>-3-phenylpropynoic acid

Downstream raw materials:

<1-13C>-(E)-methyl cinnamate

<1-13C>-(E)-cinnamic acid

<1-13C>-3-phenylpropionic acid