3-Methoxy-2-Piperidone

Base Information

Chemical Name:3-Methoxy-2-Piperidone
CAS No.:25219-59-4
Molecular Formula:C6H11NO2
Molecular Weight:129.16
Hs Code.:2933790090
Mol file:25219-59-4.mol

Synonyms:2-Piperidone,3-methoxy- (8CI);

Suppliers and Price of 3-Methoxy-2-Piperidone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Methoxypiperidin-2-one
100mg
$ 110.00

TRC
3-Methoxypiperidin-2-one
50mg
$ 65.00

SynQuest Laboratories
3-Methoxypiperidin-2-one
1 g
$ 285.00

Matrix Scientific
3-Methoxypiperidin-2-one 97%
1g
$ 360.00

Crysdot
3-Methoxypiperidin-2-one 95+%
1g
$ 201.00

Atlantic Research Chemicals
3-Methoxypiperidin-2-one 95%
1gm:
$ 233.28

Ambeed
3-Methoxypiperidin-2-one 97%
250mg
$ 52.00

Activate Scientific
3-Methoxypiperidin-2-one 95+%
5 g
$ 1170.00

Total 52 raw suppliers

Chemical Property of 3-Methoxy-2-Piperidone

Chemical Property:

Vapor Pressure:0.00389mmHg at 25°C
Refractive Index:1.461
Boiling Point:279.963 °C at 760 mmHg
PKA:15.54±0.40(Predicted)
Flash Point:123.118 °C
PSA：38.33000
Density:1.067 g/cm³
LogP:0.24020
Storage Temp.:Sealed in dry,Room Temperature

Purity/Quality:

99%, ^*data from raw suppliers

3-Methoxypiperidin-2-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses 3-Methoxypiperidin-2-one is a useful research chemical.

Technology Process of 3-Methoxy-2-Piperidone

There total 7 articles about 3-Methoxy-2-Piperidone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 67-56-1
methanol

: 463362-69-8
3-diazo-piperidin-2-one

: 25219-59-4
3-methoxy-piperidin-2-one

Guidance literature:: dirhodium tetraacetate; at 25 ℃; for 1h;
DOI:10.1016/S0040-4020(02)00278-8

Reference yield: 51.0%

: 67-56-1
methanol

: 1215765-13-1
1-chloro-3-methoxypiperidin-2-one

: 25219-59-4
3-methoxy-piperidin-2-one

: 99903-96-5
methyl 4,4-dimethoxybutylcarbamate

: 56475-88-8
methyl 2-methoxypyrrolidine-1-carboxylate

Guidance literature:: 1-chloro-3-methoxypiperidin-2-one; In dichloromethane; at -78 ℃; for 4.5h; UV-irradiation; Inert atmosphere;

methanol; With potassium carbonate; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/jo100181h

Reference yield:

: 1892-22-4,4077-38-7,34294-79-6,88763-76-2
3-aminopiperidin-2-one

: 25219-59-4
3-methoxy-piperidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / iso-amyl nitrite; glacoal AcOH / CHCl₃ / 0.25 h / Heating

2: 82 percent / Rh₂(OAc)4 / 1 h / 25 °C

With acetic acid; isopentyl nitrite; dirhodium tetraacetate; In chloroform;
DOI:10.1016/S0040-4020(02)00278-8