benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

Base Information

Chemical Name:benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate
CAS No.:121534-48-3
Molecular Formula:C₂₃H₂₄N₂O₇S
Molecular Weight:472.519
Hs Code.:

Synonyms:benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

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Chemical Property of benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

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Technology Process of benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

There total 2 articles about benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 89971-88-0
benzyl (3S,5R,6R)-6-phenoxyacetamido-penicillanate 1,1-dioxide

: 121534-48-3
benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

Guidance literature:: With 2,6-dichloro-benzonitrile; In chloroform-d1;

Reference yield:

: 1256-06-0
(2S,5R,6R)-benzyl-3,3-dimethyl-7-oxo-6-(2-phenoxyacetamido)-4-thia-1-azabicyclo[3.2.0]heptane-2-carboxylate

: 121534-48-3
benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / potassium permanganate / H₂O; acetic acid / 3.5 h / 0 °C

2: 81 percent / 30percent DBN / CDCl₃

With potassium permanganate; 2,6-dichloro-benzonitrile; In chloroform-d1; water; acetic acid;

Reference yield:

: 121534-48-3
benzyl 2-<(3S,4R)-2-oxo-3-phenoxyacetamido-4-sulphinoacetamido-4-sulphinoazetidin-1-yl>-2-methylbut-2-enoate

: 121534-50-7
benzyl 2-<(2R,3S)-2-acetonylsulphonyl-4-oxo-3-phenoxyacetamidoazetidin-1-yl>glyoxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium hydrogen carbonate, 2.) potassium iodide / 1.) EtOH, water, 0.5 h, 2.) acetone, 18 h

2: O₃ / CH₂Cl₂ / -78 °C

With sodium hydrogencarbonate; ozone; potassium iodide; In dichloromethane;