[1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

Base Information

Chemical Name:[1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide
CAS No.:1235962-13-6
Molecular Formula:Br*C₂₂H₂₄N₅O
Molecular Weight:454.369
Hs Code.:

Synonyms:[1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

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Chemical Property of [1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

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Technology Process of [1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

There total 1 articles about [1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 960205-03-2
1-mesityl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide

: 2101-87-3
p-methoxy-phenylazide

: 1235962-13-6
[1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

Guidance literature:: 1-mesityl-3-(prop-2-yn-1-yl)-1H-imidazol-3-ium bromide; With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In acetonitrile; at 60 ℃; for 1h;

p-methoxy-phenylazide; In acetonitrile; at 60 ℃; for 48h;
DOI:10.1021/om100435x

Reference yield: 93.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 1235962-13-6
[1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene-3-mesityl)imidazolium] bromide

: [1-((4-(4-methoxyphenyl)-1H-1,2,3-triazolyl)methylene)-3-mesitylimidazol-2-ylidenepalladium(II)allyl] chloride

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; (N2); ligand salt, KOC(CH3)3, and Pd complex suspended in THF, stirred for 4 h; filtered, concd. (vac.), dissolved in CH2Cl2, pptd. with pentane;
DOI:10.1021/om100435x