2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine

Base Information

• Chemical Name: 2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine
• CAS No.: 91552-24-8
• Molecular Formula: C₁₀H₁₀ClNO
• Molecular Weight: 195.648
• Mol file: 91552-24-8.mol

Synonyms:2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine

Chemical Property of 2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine

There total 1 articles about 2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

3-chloro-benzonitrile (766-84-7) + propan-1-ol-3-amine (156-87-6) → 2-(3-chlorophenyl)-5,6-dihydro-4H-1,3-oxazine (91552-24-8)

Guidance literature:

With Montmorillonite K-10; for 7h; Microwave irradiation;

DOI:10.1002/jhet.557

upstream raw materials:

3-chloro-benzonitrile

propan-1-ol-3-amine

Refernces

• 1、 Mohammadpoor-Baltork, Iraj,Moghadam, Majid,Tangestaninejad, Shahram,Mirkhani, Valiollah,Eskandari, Zohre. "Ultrasound promoted selective synthesis of 2-aryl-5,6-dihydro-4H-1,3-oxazines catalyzed by K-10 and KSF montmorillonite clays: A practical procedure under mild and solvent-free conditions". experimental part. p. 857 - 862. Retrieved 2011/10/09.