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C17H24INO

Base Information
  • Chemical Name:C17H24INO
  • CAS No.:1072091-38-3
  • Molecular Formula:C17H24INO
  • Molecular Weight:385.288
  • Hs Code.:
C<sub>17</sub>H<sub>24</sub>INO

Synonyms:C17H24INO

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Chemical Property of C17H24INO
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Technology Process of C17H24INO

There total 10 articles about C17H24INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With lithium hydroxide; mercaptoacetic acid; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h;
Guidance literature:
Multi-step reaction with 7 steps
1.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C
1.2: 8 h / 20 °C
2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C
3.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C
4.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
5.1: triethylamine / dichloromethane / 3 h / 20 °C
6.1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C
7.1: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C
With chromium dichloride; hydrogenchloride; lithium hydroxide; sulfuric acid; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
Guidance literature:
Multi-step reaction with 8 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C
2.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C
2.2: 8 h / 20 °C
3.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C
4.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C
5.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C
6.1: triethylamine / dichloromethane / 3 h / 20 °C
7.1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C
8.1: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C
With chromium dichloride; hydrogenchloride; lithium hydroxide; sulfuric acid; tetrabutyl ammonium fluoride; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
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