C₁₇H₂₄INO

Base Information Edit

Chemical Name:C₁₇H₂₄INO
CAS No.:1072091-38-3
Molecular Formula:C₁₇H₂₄INO
Molecular Weight:385.288
Hs Code.:
Mol file:1072091-38-3.mol

Synonyms:C₁₇H₂₄INO

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Chemical Property of C₁₇H₂₄INO Edit

Chemical Property:

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Technology Process of C₁₇H₂₄INO

There total 10 articles about C₁₇H₂₄INO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1072091-36-1
N-{(1S,2E)-4-(benzyloxy)-1-[(1S,2E)-3-iodo-1-methylprop-2-en-1-yl]-2-methylbut-2-en-1-yl}-N-methyl-2-nitroaniline

: 1072091-38-3
C₁₇H₂₄INO

Guidance literature:: With lithium hydroxide; mercaptoacetic acid; In N,N-dimethyl-formamide; at 20 ℃; for 2.5h;

Reference yield:

: 1072091-12-3
(2R,3S,4E)-6-(benzyloxy)-3-[(4-methoxyphenyl)amino]-2,4-dimethylhex-4-en-1-ol

: 1072091-38-3
C₁₇H₂₄INO

Guidance literature:: Multi-step reaction with 7 steps

1.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

1.2: 8 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

3.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

4.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

5.1: triethylamine / dichloromethane / 3 h / 20 °C

6.1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

7.1: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

With chromium dichloride; hydrogenchloride; lithium hydroxide; sulfuric acid; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 1072091-09-8
N-[(1S,2E)-4-(benzyloxy)-1-((1R)-2-{[tert-butyl(dimethyl)silyl]oxy}-1-methylethyl)-2-methylbut-2-en-1-yl]-4-methoxyaniline

: 1072091-38-3
C₁₇H₂₄INO

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2.1: sulfuric acid; periodic acid / water; acetonitrile / 1.5 h / 20 °C

2.2: 8 h / 20 °C

3.1: Dess-Martin periodane / dichloromethane / 0.17 h / 20 °C

4.1: chromium dichloride / tetrahydrofuran / 5.5 h / 0 - 20 °C

5.1: hydrogenchloride / ethyl acetate / 1 h / 20 °C

6.1: triethylamine / dichloromethane / 3 h / 20 °C

7.1: potassium carbonate / N,N-dimethyl-formamide / 68 h / 20 °C

8.1: lithium hydroxide; mercaptoacetic acid / N,N-dimethyl-formamide / 2.5 h / 20 °C

With chromium dichloride; hydrogenchloride; lithium hydroxide; sulfuric acid; tetrabutyl ammonium fluoride; potassium carbonate; Dess-Martin periodane; mercaptoacetic acid; periodic acid; triethylamine; In tetrahydrofuran; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;