[((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

Base Information

• Chemical Name: [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane
• CAS No.: 191216-20-3
• Molecular Formula: C₃₆H₆₆O₄Si
• Molecular Weight: 591.003

Synonyms:[((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

Chemical Property of [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

Chemical Property:

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Technology Process of [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

There total 2 articles about [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

Sorbyl alcohol (17102-64-6) + chlorotris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane (18765-53-2) → [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane (191216-20-3)

Guidance literature:

With pyridine; In toluene;

DOI:10.1021/jo970317q

Reference yield:

(-)-menthol (2216-51-5) → [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane (191216-20-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 70 percent / SiCl₄, pyridine / toluene / 4 h / 50 °C

2: 85 percent / pyridine / toluene

With pyridine; tetrachlorosilane; In toluene;

DOI:10.1021/jo970317q

Reference yield: 93.0%

4-Phenyl-1,2,4-triazolidine-3,5-dione (4233-33-4) + [((E,E)-hexa-2,4-dienyl)oxy]tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane (191216-20-3) → ({[(2,5-cis)-5-methyl-8-phenyl-7,9-dioxo-1,6,8-triaza[4.3.0]bicyclonon-3-en-2-yl]methyl}oxy)tris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

Guidance literature:

With tert-butylhypochlorite; In ethyl acetate;

DOI:10.1021/jo970317q

upstream raw materials:

Sorbyl alcohol

chlorotris(((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl)oxy)silane

(-)-menthol

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