⁽¹⁸⁾-O-chromyl chloride

Base Information

Chemical Name:⁽¹⁸⁾-O-chromyl chloride
CAS No.:238097-64-8
Molecular Formula:Cl₂CrO₂
Molecular Weight:158.902
Hs Code.:

Synonyms:⁽¹⁸⁾-O-chromyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ⁽¹⁸⁾-O-chromyl chloride

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Technology Process of ⁽¹⁸⁾-O-chromyl chloride

There total 2 articles about ⁽¹⁸⁾-O-chromyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 7782-50-5
chlorine

: 10025-73-7,16284-59-6
chromium(III) chloride

: 14797-71-8
¹⁸O-labeled water

: 238097-64-8
⁽¹⁸⁾-O-chromyl chloride

Guidance literature:: With Na; Zn; In neat (no solvent); byproducts: NaCl, H2; inert atmosphere; dissoln. of CrCl3 in H2(18)O in presence of trace Zn, freezing at -150°C, addn. of Na, stirring at room temp. overnight, treatment with Cl2 at 77 K, stirring at room temp. for 2 h, treatment with excess HCl gas for 15 min; flash fractional distn. (high vac.); contg. 70-80% (18)O;
DOI:10.1021/ic981131s