Technology Process of C14H17FO2
There total 5 articles about C14H17FO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
at 0 ℃;
for 2.5h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sulfuric acid / 4 h / 105 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C
3.1: water; sodium hydroxide / ethanol / 3 h / 55 °C
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C
4.2: 13 h / 20 °C
5.1: tetrahydrofuran / 2.5 h / 0 °C
With
sulfuric acid; water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 125 °C
2.1: water; sodium hydroxide / ethanol / 3 h / 55 °C
3.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 0.08 h / 20 °C
3.2: 13 h / 20 °C
4.1: tetrahydrofuran / 2.5 h / 0 °C
With
water; potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide;