2-Mesylbenzoyl-malonsaeurediethylester

Base Information

Chemical Name:2-Mesylbenzoyl-malonsaeurediethylester
CAS No.:75473-10-8
Molecular Formula:C₁₅H₁₈O₇S
Molecular Weight:342.37
Hs Code.:

Synonyms:2-Mesylbenzoyl-malonsaeurediethylester

Suppliers and Price of 2-Mesylbenzoyl-malonsaeurediethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Mesylbenzoyl-malonsaeurediethylester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Mesylbenzoyl-malonsaeurediethylester

There total 1 articles about 2-Mesylbenzoyl-malonsaeurediethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 49639-13-6
2-methylsulfonylbenzoyl chloride

: 105-53-3
diethyl malonate

: 75473-10-8
2-Mesylbenzoyl-malonsaeurediethylester

Guidance literature:: With tetrachloromethane; magnesium; Yield given. Multistep reaction; 1.) EtOH, ether, reflux, 3h, 2.) EtOH, ether, reflux, 10 min.;
DOI:10.1002/ardp.19803130704

Reference yield: 86.0%

: 75473-10-8
2-Mesylbenzoyl-malonsaeurediethylester

: 3323-76-0
1-(2-Methanesulfonyl-phenyl)-ethanone

Guidance literature:: With sulfuric acid; In acetic acid; for 4h; Heating;
DOI:10.1002/ardp.19803130704

Reference yield:

: 75473-10-8
2-Mesylbenzoyl-malonsaeurediethylester

: 75473-33-5
5-(2-Methanesulfonyl-phenyl)-1,3-dihydro-thieno[2,3-e][1,4]diazepin-2-one

Guidance literature:: Multi-step reaction with 8 steps

1: 86 percent / conc. H₂SO₄ / aq. acetic acid / 4 h / Heating

2: AlCl₃, Br₂ / CHCl₃

3: 78 percent / aq. ethanol / 1.5 h / 50 °C

4: 79 percent / Et₃N / dioxane / 1 h / Heating

5: K₂CO₃ / dioxane / 2 h / Ambient temperature

6: NaI / acetone / 1 h / Heating

7: conc. aq. NH₃ / CH₂Cl₂ / Ambient temperature

8: 45.5 percent / pivalic acid / 0.25 h / Heating

With ammonium hydroxide; aluminium trichloride; sulfuric acid; bromine; potassium carbonate; triethylamine; sodium iodide; Trimethylacetic acid; In 1,4-dioxane; ethanol; dichloromethane; chloroform; acetic acid; acetone;
DOI:10.1002/ardp.19803130704