dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside

Base Information

• Chemical Name: dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside
• CAS No.: 1577227-68-9
• Molecular Formula: C₂₉H₄₈O₉Si
• Molecular Weight: 568.78

Synonyms:dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside

Chemical Property of dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside

There total 3 articles about dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside (1577227-62-3) → dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside (1577227-68-9)

Guidance literature:

With toluene-4-sulfonic acid; ethanethiol; In dichloromethane; water; at 20 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c3ob42312c

Reference yield:

dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside (1577227-58-7) → dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside (1577227-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; dmap / 4 h / 0 - 20 °C / Inert atmosphere

2: ethanethiol; toluene-4-sulfonic acid / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

With pyridine; dmap; toluene-4-sulfonic acid; ethanethiol; In dichloromethane; water;

DOI:10.1039/c3ob42312c

Reference yield:

4-Acetyloxy-2,2-dimethylbutyrylchloride (107998-33-4) → dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside (1577227-68-9)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridine; dmap / 4 h / 0 - 20 °C / Inert atmosphere

2: ethanethiol; toluene-4-sulfonic acid / dichloromethane; water / 1 h / 20 °C / Inert atmosphere

With pyridine; dmap; toluene-4-sulfonic acid; ethanethiol; In dichloromethane; water;

DOI:10.1039/c3ob42312c

upstream raw materials:

dimethylthexylsilyl 3-O-benzyl-4,6-di-O-benzylidene-β-D-glucopyranoside

4-Acetyloxy-2,2-dimethylbutyrylchloride

dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-4,6-O-benzylidene-β-D-glucopyranoside

Downstream raw materials:

dimethylthexylsilyl O-methyl-2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate

C₃₉H₄₀Cl₃NO₁₂

dimethylthexylsilyl O-(methyl-2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-4-O-(9-fluorenylmethoxycarbonyl)-β-D-glucopyranosyluronate)-(1→4)-O-2-deoxy-2-azido-3-O-benzyl-6-O-acetyl-β-D-glucopyranoside

C₃₅H₃₈Cl₃NO₁₀

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 1577227-68-9 dimethylthexylsilyl 2-O-(4-acetoxy-2,2-dimethylbutanoate)-3-O-benzyl-β-D-glucopyranoside

Send

Send

Metric Ton KG G Pound L ML

Send

Send