2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

Base Information

Chemical Name:2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide
CAS No.:67019-52-7
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:

Synonyms:2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

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Chemical Property of 2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

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Technology Process of 2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

There total 6 articles about 2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 67019-55-0
2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

: 67019-52-7
2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: With tert.-butylhydroperoxide; dipyridinium dichromate; In decane; benzene; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1055/s-0035-1561583

Reference yield:

: 17159-98-7
3-(4-methoxyphenyl)-2-cyclohexen-1-one

: 67019-52-7
2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether

3: CrO₃, Py / CH₂Cl₂

With pyridine; chromium(VI) oxide; lithium aluminium tetrahydride; In diethyl ether; dichloromethane;
DOI:10.1016/0040-4020(78)88046-6

Reference yield:

: 67019-56-1
4'-methoxy-3,4,5,6-tetrahydro-[1,1'-biphenyl]-3-ol

: 67019-52-7
2-(4′-methoxy-4-oxo-1,2,3,4-tetrahydro-[1,1′-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

2: CrO₃, Py / CH₂Cl₂

With pyridine; chromium(VI) oxide; In dichloromethane;
DOI:10.1016/0040-4020(78)88046-6