2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

Base Information

Chemical Name:2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide
CAS No.:67019-55-0
Molecular Formula:C₁₇H₂₃NO₂
Molecular Weight:273.375
Hs Code.:

Synonyms:2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

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Chemical Property of 2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

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Technology Process of 2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

There total 4 articles about 2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 67019-56-1
4'-methoxy-3,4,5,6-tetrahydro-[1,1'-biphenyl]-3-ol

: 67019-55-0
2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: In para-xylene; at 200 ℃; for 0.166667h; Sealed tube; Inert atmosphere; Microwave irradiation;
DOI:10.1055/s-0035-1561583

Reference yield:

: 17159-98-7
3-(4-methoxyphenyl)-2-cyclohexen-1-one

: 67019-55-0
2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / diethyl ether

With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1016/0040-4020(78)88046-6

Reference yield:

: 117360-96-0
3-<(1-methylpropyl)oxy>-2-cyclohexen-1-one

: 67019-55-0
2-(4'-methoxy-1,2,3,4-tetrahydro-[1,1'-biphenyl]-1-yl)-N,N-dimethylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.1: cerium(III) chloride heptahydrate / methanol / 0.25 h / 20 °C / Inert atmosphere

2.2: 0.25 h / 0 °C / Inert atmosphere

3.1: para-xylene / 0.17 h / 200 °C / Sealed tube; Inert atmosphere; Microwave irradiation

With cerium(III) chloride heptahydrate; In tetrahydrofuran; methanol; para-xylene; 2.1: |Luche Cerium Reduction / 3.1: |Eschenmoser-Claisen Rearrangement;
DOI:10.1055/s-0035-1561583