2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

Base Information

Chemical Name:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)
CAS No.:131214-88-5
Molecular Formula:C₄₄H₂₀Br₈N₄Zn
Molecular Weight:1309.29
Hs Code.:

Synonyms:2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

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Chemical Property of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

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Technology Process of 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

There total 12 articles about 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 2,3,7,8,12,13,17,18-octobromo-5,10,15,20-tetraphenyl, 21H,23H-porphyrin

: 557-34-6
zinc diacetate

: 131214-88-5
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

Guidance literature:: In methanol; chloroform; H2OBP in chloroform and Zn(CH3COO)2 in methanol were mixed, stirred for 30min; solvent was evapd. under reduced pressure, residue dissolved in CHCl3, mixt. washed with water; the org. layer dried over Na2SO4; product was obtained on evapn. of the solvent; chromd. on basic alumina;

Reference yield: 30.0%

: 557-34-6
zinc diacetate

: 2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenyl-21H,23H-porphyrin

: 131214-88-5
2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato zinc(II)

Guidance literature:: In methanol; chloroform; for 3.5h; Reflux;
DOI:10.1039/c8dt02432d

Reference yield: 22.0%

: 14074-80-7
(5,10,15,20-tetraphenylporphyrinato)zinc(II)

: 7558-02-3,7758-02-3
potassium bromide

: 131214-88-5
[2,3,7,8,12,13,17,18-octabromo-5,10,15,20-tetraphenylporphyrinato]zinc

Guidance literature:: With ammonium metavanadate; perchloric acid; dihydrogen peroxide; In dichloromethane; water; at 25 ℃; for 24h; pH=1;
DOI:10.1039/c9nj02503k