S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Base Information

Chemical Name:S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine
CAS No.:173169-34-1
Molecular Formula:C₂₅H₂₆N₄O₁₁S₂
Molecular Weight:622.634
Hs Code.:

S<sup>4</sup>-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Synonyms:S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Suppliers and Price of S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

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Technology Process of S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

There total 8 articles about S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 173169-17-0
S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-3',5'-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)4-thiouridine

: 173169-34-1
S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Guidance literature:: With water; acetic acid; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; for 7h; Ambient temperature;
DOI:10.1002/hlca.19950780706

Reference yield:

: 20264-95-3
2-(4-nitrophenyl)ethyl chloride

: 173169-34-1
S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Na₂S₂O₃*5H₂O, 2.) ice, AcOH, Cl₂ gas / 1.) MeOH/water, 7-8 h, reflux, 2.) MeOH, water, 30 min

2: 70 percent / pyridine / methanol / 1.5 h / Ambient temperature

3: 82 percent / AcOH, H₂O, Et₃N*trihydrogen fluoride / tetrahydrofuran / 7 h / Ambient temperature

With pyridine; Methamphetamin; water; chlorine; sodium thiosulfate; acetic acid; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol;
DOI:10.1002/hlca.19950780706

Reference yield:

: 20264-96-4
2-(4-nitrophenyl)ethyl iodide

: 173169-34-1
S⁴-<2-(4-nitrophenyl)ethyl>-2'-O-<2-(4-nitrophenyl)ethylsulfonyl>-4-thiouridine

Guidance literature:: Multi-step reaction with 5 steps

1: 73 percent / K₂CO₃ / butan-2-one / 2.5 h / Heating

2: 85 percent / NH₃ / methanol / 20 h / Ambient temperature

3: 79 percent / pyridine / 4 h / Ambient temperature

4: 70 percent / pyridine / methanol / 1.5 h / Ambient temperature

5: 82 percent / AcOH, H₂O, Et₃N*trihydrogen fluoride / tetrahydrofuran / 7 h / Ambient temperature

With pyridine; ammonia; water; potassium carbonate; acetic acid; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol; butanone;
DOI:10.1002/hlca.19950780706