Sodium; 2-methoxy-benzenesulfinate

Base Information

• Chemical Name: Sodium; 2-methoxy-benzenesulfinate
• CAS No.: 15898-40-5
• Molecular Formula: C₇H₇O₃S*Na
• Molecular Weight: 194.187
• Mol file: 15898-40-5.mol

Synonyms:Sodium; 2-methoxy-benzenesulfinate

Chemical Property of Sodium; 2-methoxy-benzenesulfinate

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Sodium; 2-methoxy-benzenesulfinate

There total 1 articles about Sodium; 2-methoxy-benzenesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-Methoxybenzenesulfonyl chloride (10130-87-7) → Sodium; 2-methoxy-benzenesulfinate (15898-40-5)

Guidance literature:

With sodium hydrogencarbonate; sodium sulfite; In water; at 70 - 80 ℃; for 4h;

DOI:10.3184/174751914X14117977782502

Reference yield: 85.0%

bromobenzene (108-86-1,52753-63-6) + Sodium; 2-methoxy-benzenesulfinate (15898-40-5) → 1-benzenesulfonyl-2-methoxy-benzene (23038-47-3)

Guidance literature:

With pyridine; copper(I) bromide; at 80 ℃; for 12h;

DOI:10.3184/174751914X14034421692005

Reference yield: 81.0%

toluene-4-sulfonic acid phenyl ester (640-60-8) + Sodium; 2-methoxy-benzenesulfinate (15898-40-5) → 1-benzenesulfonyl-2-methoxy-benzene (23038-47-3)

Guidance literature:

With tetrakis(actonitrile)copper(I) hexafluorophosphate; In dimethyl sulfoxide; at 120 ℃;

DOI:10.3184/174751914X14117977782502

upstream raw materials:

o-Methoxybenzenesulfonyl chloride

Downstream raw materials:

2-methoxybenzene-1-sulfonyl fluoride

1-benzenesulfonyl-2-methoxy-benzene

2-(2-methoxyphenylthio)-1,4-dioxane

2,2'-Dimethoxybiphenyl