ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid

Base Information

• Chemical Name: ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid
• CAS No.: 109308-73-8
• Molecular Formula: C₁₄H₁₃Cl₂NO₆
• Molecular Weight: 362.166
• Mol file: 109308-73-8.mol

Synonyms:ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid

Chemical Property of ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid

There total 2 articles about ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl ester of (5-nitro-2,4-dichlorobenzoyl)acetic acid (174312-93-7) + orthoformic acid triethyl ester (122-51-0) → ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid (109308-73-8)

Guidance literature:

DOI:10.1007/BF02464110

Reference yield:

2,4-dichloro-5-nitro benzoyl chloride (713-28-0) → ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid (109308-73-8)

Guidance literature:

1: Acylation / 2: Substitution;

DOI:10.1007/BF02464110

Reference yield: 96.0%

ethyl ester of 2-(5-nitro-2,4-dichlorobenzoyl)-3-ethoxyacrylic acid (109308-73-8) → C14H15ClN2O6 (1176905-17-1)

Guidance literature:

With ammonia; In diethyl ether; ethanol; at 20 ℃; for 4h;

DOI:10.1021/jm701585h

upstream raw materials:

ethyl ester of (5-nitro-2,4-dichlorobenzoyl)acetic acid

orthoformic acid triethyl ester

2,4-dichloro-5-nitro benzoyl chloride

Downstream raw materials:

2-(2,4-Dichlor-5-nitro-benzoyl)-3-(2-formyl-2-methylhydrazino)acrylsaeure-ethylester

3-(Dimethylhydrazino)-2-(2,4-dichlor-5-nitrobenzoyl)-acrylsaeure-ethylester

2-(2,4-Dichlor-5-nitrobenzoyl)-3-(isopropylidenhydrazino)acrylsaeure-ethylester

(Z)-2-(2,4-Dichloro-5-nitro-benzoyl)-3-(3-fluoro-phenylamino)-acrylic acid ethyl ester