azidomanganese(III) meso-tetraphenylporphyrin

Base Information

Chemical Name:azidomanganese(III) meso-tetraphenylporphyrin
CAS No.:56413-47-9
Molecular Formula:C₄₄H₂₈MnN₇
Molecular Weight:709.691
Hs Code.:

Synonyms:azidomanganese(III) meso-tetraphenylporphyrin

Suppliers and Price of azidomanganese(III) meso-tetraphenylporphyrin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of azidomanganese(III) meso-tetraphenylporphyrin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of azidomanganese(III) meso-tetraphenylporphyrin

There total 4 articles about azidomanganese(III) meso-tetraphenylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7782-79-8
hydrogen azide

: aquahydroxo(tetraphenylporphinato)manganese(III)

: 56413-47-9
tetraphenylporphinatomanganese(III) azide

Guidance literature:: In benzene; addn. of benzene soln. of HN3 to soln. of Mn complex, stirring, 1 h; mixt. allowed to stand for 24 h; evapn. of solvent in vac., crystg. from acetone, drying in high vac. at40°C;

Reference yield:

: sodium azide

: 917-23-7,20998-75-8
5,10,15,20-tetraphenyl-21H,23H-porphine

: 638-38-0,993-02-2,2180-18-9,15411-95-7,22981-23-3,27004-39-3
manganese(II) acetate

: 56413-47-9
tetraphenylporphinatomanganese(III) azide

Guidance literature:: In N,N-dimethyl-formamide; porphyrin and 2- to 20-fold excess of Mn(AcO)2 were added to DMF, refluxed (or heated in bomb to reflux temp.) for ca. 5 h, solvent removed by high-vac. rotary evapn., extd. with mixt. of NaN3-H2O/CHCl3 by shaking for several min; aq. phase sepd., solvent removed by rotary evapn.;
DOI:10.1021/ja00323a036