1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

Base Information

Chemical Name:1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride
CAS No.:1458033-57-2
Molecular Formula:C₂₀H₂₃N₂O₃*Cl
Molecular Weight:374.867
Hs Code.:

Synonyms:1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

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Chemical Property of 1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

Chemical Property:

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Technology Process of 1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

There total 2 articles about 1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73718-62-4
3,3-dimethyl-2-methylene-1-ethyl-2,3-dihydro-1H-indole

: 2973-19-5
2-hydroxy-5-nitrobenzyl chloride

: 1458033-57-2
1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

Guidance literature:: In acetonitrile; at 20 ℃; for 6h;
DOI:10.1016/j.tet.2013.08.020

Reference yield:

: 14134-81-7
1-ethyl-2,3,3-trimethylindolium iodide

: 1458033-57-2
1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / water / 20 °C

2: acetonitrile / 6 h / 20 °C

With sodium carbonate; In water; acetonitrile;
DOI:10.1016/j.tet.2013.08.020

Reference yield:

: 1458033-57-2
1-ethyl-2-[2-(2-hydroxy-5-nitrophenyl)ethyl]-3,3-dimethyl-3H-indolium chloride

: C₂₁H₂₂N₃O₃^(1-)

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / 0.02 h

2: aq. phosphate buffer; acetonitrile / 24.84 °C / pH 7.6

With ammonium hydroxide; In aq. phosphate buffer; acetonitrile;
DOI:10.1002/open.201402117