Technology Process of C14H11FN2O4
There total 5 articles about C14H11FN2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C16H12ClFN2O5;
With
oxalyl dichloride;
N,N-dimethyl-formamide;
In
dichloromethane;
at 20 ℃;
for 3h;
With
methanol;
In
dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 1 h / Cooling with ice
2: sodium hydroxide; water / methanol / 0.5 h / Cooling with ice
3: sulfuric acid / 4 h / Cooling with ice
4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
With
oxalyl dichloride; sulfuric acid; water; sodium hydroxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 1 h / Cooling with ice
2: sodium hydroxide; water / methanol / 0.5 h / Cooling with ice
3: sulfuric acid / 4 h / Cooling with ice
4: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C
With
oxalyl dichloride; sulfuric acid; water; sodium hydroxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; methanol; dichloromethane;