benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

Base Information

Chemical Name:benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate
CAS No.:1072344-35-4
Molecular Formula:C₂₀H₃₃NO₃Si
Molecular Weight:363.572
Hs Code.:

Synonyms:benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

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Chemical Property of benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

There total 3 articles about benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 135938-63-5
2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine

: 1072344-35-4
benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 23 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ja209472h

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1072344-35-4
benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;

Reference yield:

: 3433-37-2
piperidin-2-ylmethanol

: 1072344-35-4
benzyl 2-({[tert-butyl(dimethyl)silyl]oxy}methyl)piperidine-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

2: dmap; N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

With dmap; N-ethyl-N,N-diisopropylamine; In dichloromethane;