tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

Base Information

Chemical Name:tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate
CAS No.:1072344-54-7
Molecular Formula:C₁₉H₂₆N₂O₅S
Molecular Weight:394.492
Hs Code.:

Synonyms:tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

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Chemical Property of tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

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Technology Process of tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

There total 7 articles about tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1072344-48-9
tert-butyl (piperidin-2-ylmethoxy)acetate

: 69360-26-5
2-cyanobenzenesulfonyl chloride

: 1072344-54-7
tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

Guidance literature:: With potassium carbonate; In water; 1,2-dichloro-ethane; at 20 ℃;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1072344-54-7
tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / tetra-(n-butyl)ammonium iodide / water; toluene / 0 - 20 °C

2: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

3: potassium carbonate / water; 1,2-dichloro-ethane / 20 °C

With sodium hydroxide; hydrogen; potassium carbonate; palladium 10% on activated carbon; tetra-(n-butyl)ammonium iodide; In ethanol; water; 1,2-dichloro-ethane; toluene;

Reference yield:

: 1072344-41-2
benzyl 2-[(2-tert-butoxy-2-oxoethoxy)methyl]piperidine-1-carboxylate

: 1072344-54-7
tert-butyl ({1-[(2-cyanophenyl)sulfonyl]piperidin-2-yl}methoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 20 °C

2: potassium carbonate / water; 1,2-dichloro-ethane / 20 °C

With hydrogen; potassium carbonate; palladium 10% on activated carbon; In ethanol; water; 1,2-dichloro-ethane;