(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

Base Information

Chemical Name:(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester
CAS No.:625093-88-1
Molecular Formula:C₁₂H₁₅F₃NO₅P
Molecular Weight:341.224
Hs Code.:

Synonyms:(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

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Chemical Property of (1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

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Technology Process of (1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

There total 3 articles about (1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₂₃F₃NO₅PSi

: 625093-88-1
(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

Guidance literature:: With bicarbonate; citric acid; In water;
DOI:10.1021/jo034229j

Reference yield:

: 17049-78-4
trifluoro-acetic acid 1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl ester

: 625093-88-1
(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / CH₂Cl₂

2: citric acid; bicarbonate / H₂O

With pyridine; bicarbonate; citric acid; In dichloromethane; water;
DOI:10.1021/jo034229j

Reference yield:

: 21646-99-1
diphosphorous acid tetraethyl ester

: 6798-33-0
1-(benzyloxycarbonylamino)-2,2,2-trifluoroethanol

: 868-85-9
Dimethyl phosphite

: 625093-88-1
(1-benzyloxycarbonylamino-2,2,2-trifluoro-ethyl)-phosphonic acid dimethyl ester

: 625093-77-8
diethyl {1-[(benzyloxycarbonyl)amino]-2,2,2-trifluoroethyl}phosphonate

Guidance literature:: diphosphorous acid tetraethyl ester; 1-(benzyloxycarbonylamino)-2,2,2-trifluoroethanol; With pyridine; In dichloromethane; for 0.166667h;

Dimethyl phosphite; In dichloromethane;
DOI:10.1021/jo034229j