(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

Base Information

Chemical Name:(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol
CAS No.:1388825-54-4
Molecular Formula:C₂₄H₂₆N₂OS
Molecular Weight:390.549
Hs Code.:

Synonyms:(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

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Technology Process of (Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

There total 9 articles about (Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1388824-77-8
(Z)-4-(1-(6-chloropyridin-3-yl)-2-phenylbut-1-enyl)phenol

: 33744-33-1
β-methylaminoethanethiol hydrochloride

: 1388825-54-4
(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

Guidance literature:: β-methylaminoethanethiol hydrochloride; With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 1h;

(Z)-4-(1-(6-chloropyridin-3-yl)-2-phenylbut-1-enyl)phenol; In tetrahydrofuran; for 48h; Reflux;

Reference yield:

: 99522-34-6
4-[(tetrahydro-2H-pyran-2-yl)oxy]iodobenzene

: 1388825-54-4
(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 °C / Inert atmosphere

2.1: zinc; titanium tetrachloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

3.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

3.2: 48 h / Reflux

With n-butyllithium; titanium tetrachloride; sodium hydride; zinc; In tetrahydrofuran; 2.1: |McMurry Reaction;

Reference yield:

: 93-55-0
1-phenyl-propan-1-one

: 1388825-54-4
(Z)-4-(1-(6-(2-(methylamino)ethylthio)pyridin-3-yl)-2-phenylbut-1-enyl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; titanium tetrachloride / tetrahydrofuran / 2 h / Inert atmosphere; Reflux

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C

2.2: 48 h / Reflux

With titanium tetrachloride; sodium hydride; zinc; In tetrahydrofuran; 1.1: |McMurry Reaction;