2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

Base Information

Chemical Name:2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside
CAS No.:1000813-71-7
Molecular Formula:C₃₅H₃₂N₂O₁₂
Molecular Weight:672.645
Hs Code.:

Synonyms:2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

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Chemical Property of 2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

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Technology Process of 2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

There total 1 articles about 2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 20770-84-7,113566-69-1,113566-70-4
2,3-di-O-benzyl-4,6-O-benzylidene-α/β-D-mannopyranose

: 367946-80-3
methyl 2-fluoro-3,5-dinitrobenzoic ester

: 1000813-71-7
2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

Guidance literature:: With dmap; lithium carbonate; In dichloromethane; for 1h;
DOI:10.1080/07328300701634762

Reference yield: 80.0%

: 67-56-1
methanol

: 1000813-71-7
2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

: methyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

Guidance literature:: at 130 ℃; for 20h;
DOI:10.1080/07328300701634762

Reference yield: 74.0%

: 1000813-71-7
2,4-dinitro-6-(methoxycarbonyl)phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranoside

: 4064-06-6
1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

: 6-O-[2,3-di-O-benzyl-4,6-O-benzylidene-α/β-D-mannopyranosyl]-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

Guidance literature:: With 3 A molecular sieve; lithium perchlorate; In dichloromethane; at 150 ℃; for 1h; microwave irradiation;
DOI:10.1080/07328300701634762