methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

Base Information

Chemical Name:methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)
CAS No.:263720-29-2
Molecular Formula:C₄₀H₄₀N₂O₆
Molecular Weight:644.767
Hs Code.:

Synonyms:methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

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Chemical Property of methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

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Technology Process of methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

There total 5 articles about methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 244138-64-5
(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-2-iodo-5,6,7,8-tetrahydroimidazo[1,2-a]pyridine

: 263720-29-2
methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

Guidance literature:: With Pd(OAc)2[P(2-tolyl)3]2; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 2h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<58::AID-HLCA58>3.0.CO;2-K

Reference yield: 17.0%

: 5518-52-5
trifuran-2-yl-phosphane

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 244138-64-5
(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-2-iodo-5,6,7,8-tetrahydroimidazo[1,2-a]pyridine

: 263720-29-2
methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

: {(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}tris[furan-2-yl]phosphonium chloride

Guidance literature:: With palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<58::AID-HLCA58>3.0.CO;2-K

Reference yield: 13.0%

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 603-35-0
triphenylphosphine

: 244138-64-5
(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-2-iodo-5,6,7,8-tetrahydroimidazo[1,2-a]pyridine

: 263720-29-2
methyl (E-3{(5R,6R,7S,8S)-6,7,8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}prop-2-enoate)

: triphenyl{(5R,6R,7S,8S)-6,7-8-tris(benzyloxy)-5-[(benzyloxy)methyl]-5,6,7,8-tetrahydroimidazo[1,2-a]pyridin-2-yl}phosphonium chloride

Guidance literature:: With palladium diacetate; potassium carbonate; In N,N-dimethyl-formamide; at 80 ℃; for 8h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<58::AID-HLCA58>3.0.CO;2-K